.. _sec.units.granulator: Granulator ========== This unit represents a simplified model of a fluidized bed granulation reactor. The model does not take into account attrition of particles inside the apparatus and does not keep properly any secondary distributed properties except size. Continuous granulator ^^^^^^^^^^^^^^^^^^^^^ .. image:: ../static/images/003_models/granulator.png :width: 500px :alt: :align: center .. math:: \frac{dq_{3,i}}{dt} = -G_e\,\frac{q_{3,i} - q_{3,i-1}\,\left(\frac{d_{p,i}}{d_{p,i-1}}\right)^3}{\Delta d_i} + \frac{\dot{m}_{in}}{M_{tot}}\,q_{3,i}^{in} - \frac{\dot{m}_{out}}{M_{tot}}\,q_{3,i} .. math:: G_e = \frac{2\dot{m}_e}{\rho_{s,susp} \cdot A_{tot}} .. math:: A_{tot} = \frac{6M_{tot}}{\rho_s} \sum\limits_{i} \frac{q_{3,i}\cdot \Delta d_i}{d_{p,i}} .. math:: \dot{m}_e = \dot{m}_{s,susp}\,(1 - K_{os}) .. math:: \dot{m}_{out} = \dot{m}_{in} + \dot{m}_{e} .. math:: \dot{m}_{dust} = \dot{m}_{s,susp}\cdot K_{os} + (\dot{m}_{susp} - \dot{m}_{s,susp} + \dot{m}_{fl,g}) Batch granulator ^^^^^^^^^^^^^^^^^^^^^ .. image:: ../static/images/003_models/granulator_batch.png :width: 500px :alt: :align: center .. math:: \frac{d(M_{tot}q_{3,i})}{dt} = -G_e\,\frac{M_{tot}q_{3,i} - M_{tot}q_{3,i-1}\,\left(\frac{d_{p,i}}{d_{p,i-1}}\right)^3}{\Delta d_i} .. math:: G_e = \frac{2\dot{m}_{s,susp}}{\rho_{s,susp} \cdot A_{tot}} .. math:: A_{tot} = \frac{6M_{tot}}{\rho_s} \sum\limits_{i} \frac{q_{3,i}\cdot \Delta d_i}{d_{p,i}} .. math:: \frac{dM_{tot}}{dt} = \dot{m}_{s,susp} .. math:: \dot{m}_{exh} = \dot{m}_{l,susp} + \dot{m}_{fl,gas} .. note:: Notations: :math:`q_3` – mass density distribution of particles inside apparatus :math:`q_3^{in}` – mass density distribution of external particles from **ExternalNuclei** stream :math:`\Delta d` – class size :math:`d_p` – particle diameter in a class :math:`\dot{m}_{in}` – mass flow of input nuclei :math:`\dot{m}_{out}` – output mass flow of the product :math:`\dot{m}_{dust}` – output mass flow from the **DustOutput** :math:`\dot{m}_{susp}` – total mass flow of the suspension :math:`\dot{m}_{s,susp}` – mass flow of the solid phase in the **Suspension** inlet :math:`\dot{m}_{fl,g}` – mass flow of the gas phase in the **FluidizationGas** inlet :math:`\dot{m}_{exh}` – output mass flow from the **ExhaustGasOutput** :math:`\dot{m}_{e}` – effective mass stream of the injected suspension :math:`M_{tot}` – holdup mass :math:`\rho_{s,susp}` – density of solids in the holdup :math:`G_{e}` – effective growth rate :math:`A_{tot}` – total surface of particles in the granulator :math:`K_{os}` – overspray part in the suspension .. note:: particle size distribution is required for the simulation. This unit is applied for solid, liquid and gas phases. .. note:: Input parameters needed for the simulation: +------+-----------------+----------------------------------------+-------+--------------+ | Name | Symbol | Description | Units | Boundaries | +======+=================+========================================+=======+==============+ | Kos | :math:`K_{os}` | Overspray part in the suspension | [--] | 0 ≤ Kos ≤ 1 | +------+-----------------+----------------------------------------+-------+--------------+ | RTol | -- | Relative tolerance for equation solver | [--] | 0 < RTol ≤ 1 | +------+-----------------+----------------------------------------+-------+--------------+ | ATol | -- | Absolute tolerance for equation solver | [--] | 0 < ATol ≤ 1 | +------+-----------------+----------------------------------------+-------+--------------+ .. note:: State variables: +-------+-----------------------+-----------------------------------------------+-----------------+ | Name | Symbol | Description | Units | +=======+=======================+===============================================+=================+ | Atot | :math:`A_{tot}` | Total surface of particles in the granulator | [:math:`m^2`] | +-------+-----------------------+-----------------------------------------------+-----------------+ | Mtot | :math:`M_{tot}` | Total mass of all particles in the granulator | [kg] | +-------+-----------------------+-----------------------------------------------+-----------------+ | Mout | :math:`\dot{m}_{out}` | Output mass flow of the product | [kg/s] | +-------+-----------------------+-----------------------------------------------+-----------------+ | Mdust | :math:`\dot{m}_{dust}`| Output mass flow of dust | [kg/s] | +-------+-----------------------+-----------------------------------------------+-----------------+ | G | :math:`G_{e}` | Effective growth rate | [m/s] | +-------+-----------------------+-----------------------------------------------+-----------------+ | PSDi | :math:`q_{3,i}` | Mass density distribution of particles | [1/m] | +-------+-----------------------+-----------------------------------------------+-----------------+ .. seealso:: a demostration file at ``Example Flowsheets/Units/Granulator.dlfw``. .. seealso:: S.Heinrich, M. Peglow, M. Ihlow, M. Henneberg, L. Mörl, Analysis of the start-up process in continuous fluidized bed spray granulation by population balance modelling, Chem. Eng. Sci. 57 (2002) 4369-4390. |